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5-methyl-2-hexanone  (Millipore)


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    Millipore 5-methyl-2-hexanone
    5 Methyl 2 Hexanone, supplied by Millipore, used in various techniques. Bioz Stars score: 90/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
    https://www.bioz.com/product/5-methyl-2-hexanone/5+methyl+2+hexanone/pmc09243525__mmc2-306-58-59
    Average 90 stars, based on 1 article reviews
    5-methyl-2-hexanone - by Bioz Stars, 2026-10
    90/100 stars

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    Recombinant:

    Article Title: Pressurised liquid extraction of volatile compounds in coffee bean
    Article Snippet: In this work, we reported a novel application of pressurised liquid extraction (PLE) on coffee bean.. The condition of PLE was carefully optimised with the aid of response surface methodology (RSM) including adjustment of experimental parameters (solvent type and sample to hydromatrix ratio) and other operating parameters (i.e. temperature (50–100 1C), pressure (1000–2000 psi) and static extraction time (5–15 min)).. The coffee extracts obtained under three different extraction conditions were evaluated through descriptive sensory analysis.

    Article Title: A behavioral paradigm for measuring perceptual distances in mice
    Article Snippet: 5-Methyl-2-Hexanone , Sigma-Aldrich , 537,705-1L.

    Article Title: Prefrontal Pathways Provide Top-Down Control of Memory for Sequences of Events
    Article Snippet: 5-Methyl-2-Hexanone , Sigma-Aldrich , CAS: 110-12-3.

    Article Title: A behavioral paradigm for measuring perceptual distances in mice
    Article Snippet: REAGENT or RESOURCE SOURCE IDENTIFIER Chemicals, peptides, and recombinant proteins Cinnamaldehyde Sigma-Aldrich C80687-25G Ethyl butyrate Sigma-Aldrich E15701-500ML 2-Methylbutyric acid Sigma-Aldrich 193,070-25G 2,2-Dimethylbutyric acid Oakwood Chemical 035,602-5g Cyclopentanecarboxylic acid Sigma-Aldrich 537,683-100ML 2-Heptanone Sigma-Aldrich 537,683-100ML Isobutyric acid Sigma-Aldrich I1754-100ML Isovaleric acid Sigma-Aldrich 129,542-100ML 3-Heptanone TCI H0038 Methylvalerate Sigma-Aldrich 277,827-5G Propionic acid Sigma-Aldrich 81,910-1L Butyric acid Sigma-Aldrich B103500-100ML (+)-a-Pinene Sigma-Aldrich P45680-100ML Benzaldehyde Sigma-Aldrich B1334-100G 5-Methyl-2-Hexanone Sigma-Aldrich 537,705-1L Valeric acid Sigma-Aldrich 110,140-1L 3-Methylvaleric acid Sigma-Aldrich 222,453-5G 3,3-Dimethylbutyric acid Sigma-Aldrich B88403-25G 4-Methylvaleric acid Sigma-Aldrich 277,827-5G Hexanoic acid Sigma-Aldrich 153,745-2.5G Experimental models: Organisms/strains Mouse: C57BL/6J-Tg(Thy1-GCaMP6f) GP5.11Dkim/J The Jackson Laboratory Strain #:024,339 Deposited data Mouse behavioral data This paper http://github.com/pyrfume/pyrfume-data Software and algorithms Python version 3.8 Python Software Foundation https://www.python.org Voeyur software Smear et al., 2013 https://github.com/olfa-lab/Voyeur Multidimensional scaling Borg and Groenen, 1997, Kruskal, 1964a https://scikit-learn.org/stable/modules/ generated/sklearn.manifold.MDS.html Code for manuscript http://github.com/olfa-lab/ mouse-perceptual-distance https://doi.org/10.5281/zenodo.6537497 Other Arduino Mega 2560 microcontroller Arduino https://www.arduino.cc Mass flow controller (0–1000 mL/min) Alicat Alicat MC-1SLPM-D/5M/5IN Mass flow controller (0–100 mL/min) Alicat MC-100SCCM-D/5M/5IN Inline manifold isolation valve NResearch 225T082 2-way normally closed isolation valve NResearch TI1403270 3-way isolation valve NResearch SH360T042 Precleaned Volatile Organic Analyte (VOA) Sampling Vials Restek 21,797 Capacitive touch sensor Sparkfun SEN-1024 Pinch valve Valcor SV74P61T e1 Cell Reports Methods 2, 100233, June 20, 2022 Report ll OPEN ACCESS


    Article Title: Monitoring the oxidation of almond oils by HS-SPME–GC–MS and ATR-FTIR: Application of volatile compounds determination to cultivar authenticity
    Article Snippet: In this study, the oxidative process of Spanish and American almond oils was monitored by using headspace solid-phase microextraction/gas chromatography–mass spectrometry (HS-SPME/GC–MS) and attenuated total reflectance Fourier transform infrared spectroscopy (ATR-FTIR).. Oxidative stability of samples was evaluated after thermal treatment at 100 C for 1, 3, 5, 7, 10, 15 and 20 days, in order to accelerate the lipid oxidation process.. Variations observed in bands of infrared spectra were used to monitor the progress of the oxidation process of almond oils.

    Software:

    Article Title: Pressurised liquid extraction of volatile compounds in coffee bean
    Article Snippet: In this work, we reported a novel application of pressurised liquid extraction (PLE) on coffee bean.. The condition of PLE was carefully optimised with the aid of response surface methodology (RSM) including adjustment of experimental parameters (solvent type and sample to hydromatrix ratio) and other operating parameters (i.e. temperature (50–100 1C), pressure (1000–2000 psi) and static extraction time (5–15 min)).. The coffee extracts obtained under three different extraction conditions were evaluated through descriptive sensory analysis.

    Article Title: A behavioral paradigm for measuring perceptual distances in mice
    Article Snippet: 5-Methyl-2-Hexanone , Sigma-Aldrich , 537,705-1L.

    Article Title: Prefrontal Pathways Provide Top-Down Control of Memory for Sequences of Events
    Article Snippet: 5-Methyl-2-Hexanone , Sigma-Aldrich , CAS: 110-12-3.

    Article Title: A behavioral paradigm for measuring perceptual distances in mice
    Article Snippet: REAGENT or RESOURCE SOURCE IDENTIFIER Chemicals, peptides, and recombinant proteins Cinnamaldehyde Sigma-Aldrich C80687-25G Ethyl butyrate Sigma-Aldrich E15701-500ML 2-Methylbutyric acid Sigma-Aldrich 193,070-25G 2,2-Dimethylbutyric acid Oakwood Chemical 035,602-5g Cyclopentanecarboxylic acid Sigma-Aldrich 537,683-100ML 2-Heptanone Sigma-Aldrich 537,683-100ML Isobutyric acid Sigma-Aldrich I1754-100ML Isovaleric acid Sigma-Aldrich 129,542-100ML 3-Heptanone TCI H0038 Methylvalerate Sigma-Aldrich 277,827-5G Propionic acid Sigma-Aldrich 81,910-1L Butyric acid Sigma-Aldrich B103500-100ML (+)-a-Pinene Sigma-Aldrich P45680-100ML Benzaldehyde Sigma-Aldrich B1334-100G 5-Methyl-2-Hexanone Sigma-Aldrich 537,705-1L Valeric acid Sigma-Aldrich 110,140-1L 3-Methylvaleric acid Sigma-Aldrich 222,453-5G 3,3-Dimethylbutyric acid Sigma-Aldrich B88403-25G 4-Methylvaleric acid Sigma-Aldrich 277,827-5G Hexanoic acid Sigma-Aldrich 153,745-2.5G Experimental models: Organisms/strains Mouse: C57BL/6J-Tg(Thy1-GCaMP6f) GP5.11Dkim/J The Jackson Laboratory Strain #:024,339 Deposited data Mouse behavioral data This paper http://github.com/pyrfume/pyrfume-data Software and algorithms Python version 3.8 Python Software Foundation https://www.python.org Voeyur software Smear et al., 2013 https://github.com/olfa-lab/Voyeur Multidimensional scaling Borg and Groenen, 1997, Kruskal, 1964a https://scikit-learn.org/stable/modules/ generated/sklearn.manifold.MDS.html Code for manuscript http://github.com/olfa-lab/ mouse-perceptual-distance https://doi.org/10.5281/zenodo.6537497 Other Arduino Mega 2560 microcontroller Arduino https://www.arduino.cc Mass flow controller (0–1000 mL/min) Alicat Alicat MC-1SLPM-D/5M/5IN Mass flow controller (0–100 mL/min) Alicat MC-100SCCM-D/5M/5IN Inline manifold isolation valve NResearch 225T082 2-way normally closed isolation valve NResearch TI1403270 3-way isolation valve NResearch SH360T042 Precleaned Volatile Organic Analyte (VOA) Sampling Vials Restek 21,797 Capacitive touch sensor Sparkfun SEN-1024 Pinch valve Valcor SV74P61T e1 Cell Reports Methods 2, 100233, June 20, 2022 Report ll OPEN ACCESS


    Article Title: Monitoring the oxidation of almond oils by HS-SPME–GC–MS and ATR-FTIR: Application of volatile compounds determination to cultivar authenticity
    Article Snippet: In this study, the oxidative process of Spanish and American almond oils was monitored by using headspace solid-phase microextraction/gas chromatography–mass spectrometry (HS-SPME/GC–MS) and attenuated total reflectance Fourier transform infrared spectroscopy (ATR-FTIR).. Oxidative stability of samples was evaluated after thermal treatment at 100 C for 1, 3, 5, 7, 10, 15 and 20 days, in order to accelerate the lipid oxidation process.. Variations observed in bands of infrared spectra were used to monitor the progress of the oxidation process of almond oils.

    Generated:

    Article Title: Pressurised liquid extraction of volatile compounds in coffee bean
    Article Snippet: In this work, we reported a novel application of pressurised liquid extraction (PLE) on coffee bean.. The condition of PLE was carefully optimised with the aid of response surface methodology (RSM) including adjustment of experimental parameters (solvent type and sample to hydromatrix ratio) and other operating parameters (i.e. temperature (50–100 1C), pressure (1000–2000 psi) and static extraction time (5–15 min)).. The coffee extracts obtained under three different extraction conditions were evaluated through descriptive sensory analysis.

    Article Title: A behavioral paradigm for measuring perceptual distances in mice
    Article Snippet: 5-Methyl-2-Hexanone , Sigma-Aldrich , 537,705-1L.

    Article Title: Prefrontal Pathways Provide Top-Down Control of Memory for Sequences of Events
    Article Snippet: 5-Methyl-2-Hexanone , Sigma-Aldrich , CAS: 110-12-3.

    Article Title: A behavioral paradigm for measuring perceptual distances in mice
    Article Snippet: REAGENT or RESOURCE SOURCE IDENTIFIER Chemicals, peptides, and recombinant proteins Cinnamaldehyde Sigma-Aldrich C80687-25G Ethyl butyrate Sigma-Aldrich E15701-500ML 2-Methylbutyric acid Sigma-Aldrich 193,070-25G 2,2-Dimethylbutyric acid Oakwood Chemical 035,602-5g Cyclopentanecarboxylic acid Sigma-Aldrich 537,683-100ML 2-Heptanone Sigma-Aldrich 537,683-100ML Isobutyric acid Sigma-Aldrich I1754-100ML Isovaleric acid Sigma-Aldrich 129,542-100ML 3-Heptanone TCI H0038 Methylvalerate Sigma-Aldrich 277,827-5G Propionic acid Sigma-Aldrich 81,910-1L Butyric acid Sigma-Aldrich B103500-100ML (+)-a-Pinene Sigma-Aldrich P45680-100ML Benzaldehyde Sigma-Aldrich B1334-100G 5-Methyl-2-Hexanone Sigma-Aldrich 537,705-1L Valeric acid Sigma-Aldrich 110,140-1L 3-Methylvaleric acid Sigma-Aldrich 222,453-5G 3,3-Dimethylbutyric acid Sigma-Aldrich B88403-25G 4-Methylvaleric acid Sigma-Aldrich 277,827-5G Hexanoic acid Sigma-Aldrich 153,745-2.5G Experimental models: Organisms/strains Mouse: C57BL/6J-Tg(Thy1-GCaMP6f) GP5.11Dkim/J The Jackson Laboratory Strain #:024,339 Deposited data Mouse behavioral data This paper http://github.com/pyrfume/pyrfume-data Software and algorithms Python version 3.8 Python Software Foundation https://www.python.org Voeyur software Smear et al., 2013 https://github.com/olfa-lab/Voyeur Multidimensional scaling Borg and Groenen, 1997, Kruskal, 1964a https://scikit-learn.org/stable/modules/ generated/sklearn.manifold.MDS.html Code for manuscript http://github.com/olfa-lab/ mouse-perceptual-distance https://doi.org/10.5281/zenodo.6537497 Other Arduino Mega 2560 microcontroller Arduino https://www.arduino.cc Mass flow controller (0–1000 mL/min) Alicat Alicat MC-1SLPM-D/5M/5IN Mass flow controller (0–100 mL/min) Alicat MC-100SCCM-D/5M/5IN Inline manifold isolation valve NResearch 225T082 2-way normally closed isolation valve NResearch TI1403270 3-way isolation valve NResearch SH360T042 Precleaned Volatile Organic Analyte (VOA) Sampling Vials Restek 21,797 Capacitive touch sensor Sparkfun SEN-1024 Pinch valve Valcor SV74P61T e1 Cell Reports Methods 2, 100233, June 20, 2022 Report ll OPEN ACCESS


    Article Title: Monitoring the oxidation of almond oils by HS-SPME–GC–MS and ATR-FTIR: Application of volatile compounds determination to cultivar authenticity
    Article Snippet: In this study, the oxidative process of Spanish and American almond oils was monitored by using headspace solid-phase microextraction/gas chromatography–mass spectrometry (HS-SPME/GC–MS) and attenuated total reflectance Fourier transform infrared spectroscopy (ATR-FTIR).. Oxidative stability of samples was evaluated after thermal treatment at 100 C for 1, 3, 5, 7, 10, 15 and 20 days, in order to accelerate the lipid oxidation process.. Variations observed in bands of infrared spectra were used to monitor the progress of the oxidation process of almond oils.

    Isolation:

    Article Title: Pressurised liquid extraction of volatile compounds in coffee bean
    Article Snippet: In this work, we reported a novel application of pressurised liquid extraction (PLE) on coffee bean.. The condition of PLE was carefully optimised with the aid of response surface methodology (RSM) including adjustment of experimental parameters (solvent type and sample to hydromatrix ratio) and other operating parameters (i.e. temperature (50–100 1C), pressure (1000–2000 psi) and static extraction time (5–15 min)).. The coffee extracts obtained under three different extraction conditions were evaluated through descriptive sensory analysis.

    Article Title: A behavioral paradigm for measuring perceptual distances in mice
    Article Snippet: 5-Methyl-2-Hexanone , Sigma-Aldrich , 537,705-1L.

    Article Title: Prefrontal Pathways Provide Top-Down Control of Memory for Sequences of Events
    Article Snippet: 5-Methyl-2-Hexanone , Sigma-Aldrich , CAS: 110-12-3.

    Article Title: A behavioral paradigm for measuring perceptual distances in mice
    Article Snippet: REAGENT or RESOURCE SOURCE IDENTIFIER Chemicals, peptides, and recombinant proteins Cinnamaldehyde Sigma-Aldrich C80687-25G Ethyl butyrate Sigma-Aldrich E15701-500ML 2-Methylbutyric acid Sigma-Aldrich 193,070-25G 2,2-Dimethylbutyric acid Oakwood Chemical 035,602-5g Cyclopentanecarboxylic acid Sigma-Aldrich 537,683-100ML 2-Heptanone Sigma-Aldrich 537,683-100ML Isobutyric acid Sigma-Aldrich I1754-100ML Isovaleric acid Sigma-Aldrich 129,542-100ML 3-Heptanone TCI H0038 Methylvalerate Sigma-Aldrich 277,827-5G Propionic acid Sigma-Aldrich 81,910-1L Butyric acid Sigma-Aldrich B103500-100ML (+)-a-Pinene Sigma-Aldrich P45680-100ML Benzaldehyde Sigma-Aldrich B1334-100G 5-Methyl-2-Hexanone Sigma-Aldrich 537,705-1L Valeric acid Sigma-Aldrich 110,140-1L 3-Methylvaleric acid Sigma-Aldrich 222,453-5G 3,3-Dimethylbutyric acid Sigma-Aldrich B88403-25G 4-Methylvaleric acid Sigma-Aldrich 277,827-5G Hexanoic acid Sigma-Aldrich 153,745-2.5G Experimental models: Organisms/strains Mouse: C57BL/6J-Tg(Thy1-GCaMP6f) GP5.11Dkim/J The Jackson Laboratory Strain #:024,339 Deposited data Mouse behavioral data This paper http://github.com/pyrfume/pyrfume-data Software and algorithms Python version 3.8 Python Software Foundation https://www.python.org Voeyur software Smear et al., 2013 https://github.com/olfa-lab/Voyeur Multidimensional scaling Borg and Groenen, 1997, Kruskal, 1964a https://scikit-learn.org/stable/modules/ generated/sklearn.manifold.MDS.html Code for manuscript http://github.com/olfa-lab/ mouse-perceptual-distance https://doi.org/10.5281/zenodo.6537497 Other Arduino Mega 2560 microcontroller Arduino https://www.arduino.cc Mass flow controller (0–1000 mL/min) Alicat Alicat MC-1SLPM-D/5M/5IN Mass flow controller (0–100 mL/min) Alicat MC-100SCCM-D/5M/5IN Inline manifold isolation valve NResearch 225T082 2-way normally closed isolation valve NResearch TI1403270 3-way isolation valve NResearch SH360T042 Precleaned Volatile Organic Analyte (VOA) Sampling Vials Restek 21,797 Capacitive touch sensor Sparkfun SEN-1024 Pinch valve Valcor SV74P61T e1 Cell Reports Methods 2, 100233, June 20, 2022 Report ll OPEN ACCESS


    Article Title: Monitoring the oxidation of almond oils by HS-SPME–GC–MS and ATR-FTIR: Application of volatile compounds determination to cultivar authenticity
    Article Snippet: In this study, the oxidative process of Spanish and American almond oils was monitored by using headspace solid-phase microextraction/gas chromatography–mass spectrometry (HS-SPME/GC–MS) and attenuated total reflectance Fourier transform infrared spectroscopy (ATR-FTIR).. Oxidative stability of samples was evaluated after thermal treatment at 100 C for 1, 3, 5, 7, 10, 15 and 20 days, in order to accelerate the lipid oxidation process.. Variations observed in bands of infrared spectra were used to monitor the progress of the oxidation process of almond oils.

    Sampling:

    Article Title: Pressurised liquid extraction of volatile compounds in coffee bean
    Article Snippet: In this work, we reported a novel application of pressurised liquid extraction (PLE) on coffee bean.. The condition of PLE was carefully optimised with the aid of response surface methodology (RSM) including adjustment of experimental parameters (solvent type and sample to hydromatrix ratio) and other operating parameters (i.e. temperature (50–100 1C), pressure (1000–2000 psi) and static extraction time (5–15 min)).. The coffee extracts obtained under three different extraction conditions were evaluated through descriptive sensory analysis.

    Article Title: A behavioral paradigm for measuring perceptual distances in mice
    Article Snippet: 5-Methyl-2-Hexanone , Sigma-Aldrich , 537,705-1L.

    Article Title: Prefrontal Pathways Provide Top-Down Control of Memory for Sequences of Events
    Article Snippet: 5-Methyl-2-Hexanone , Sigma-Aldrich , CAS: 110-12-3.

    Article Title: A behavioral paradigm for measuring perceptual distances in mice
    Article Snippet: REAGENT or RESOURCE SOURCE IDENTIFIER Chemicals, peptides, and recombinant proteins Cinnamaldehyde Sigma-Aldrich C80687-25G Ethyl butyrate Sigma-Aldrich E15701-500ML 2-Methylbutyric acid Sigma-Aldrich 193,070-25G 2,2-Dimethylbutyric acid Oakwood Chemical 035,602-5g Cyclopentanecarboxylic acid Sigma-Aldrich 537,683-100ML 2-Heptanone Sigma-Aldrich 537,683-100ML Isobutyric acid Sigma-Aldrich I1754-100ML Isovaleric acid Sigma-Aldrich 129,542-100ML 3-Heptanone TCI H0038 Methylvalerate Sigma-Aldrich 277,827-5G Propionic acid Sigma-Aldrich 81,910-1L Butyric acid Sigma-Aldrich B103500-100ML (+)-a-Pinene Sigma-Aldrich P45680-100ML Benzaldehyde Sigma-Aldrich B1334-100G 5-Methyl-2-Hexanone Sigma-Aldrich 537,705-1L Valeric acid Sigma-Aldrich 110,140-1L 3-Methylvaleric acid Sigma-Aldrich 222,453-5G 3,3-Dimethylbutyric acid Sigma-Aldrich B88403-25G 4-Methylvaleric acid Sigma-Aldrich 277,827-5G Hexanoic acid Sigma-Aldrich 153,745-2.5G Experimental models: Organisms/strains Mouse: C57BL/6J-Tg(Thy1-GCaMP6f) GP5.11Dkim/J The Jackson Laboratory Strain #:024,339 Deposited data Mouse behavioral data This paper http://github.com/pyrfume/pyrfume-data Software and algorithms Python version 3.8 Python Software Foundation https://www.python.org Voeyur software Smear et al., 2013 https://github.com/olfa-lab/Voyeur Multidimensional scaling Borg and Groenen, 1997, Kruskal, 1964a https://scikit-learn.org/stable/modules/ generated/sklearn.manifold.MDS.html Code for manuscript http://github.com/olfa-lab/ mouse-perceptual-distance https://doi.org/10.5281/zenodo.6537497 Other Arduino Mega 2560 microcontroller Arduino https://www.arduino.cc Mass flow controller (0–1000 mL/min) Alicat Alicat MC-1SLPM-D/5M/5IN Mass flow controller (0–100 mL/min) Alicat MC-100SCCM-D/5M/5IN Inline manifold isolation valve NResearch 225T082 2-way normally closed isolation valve NResearch TI1403270 3-way isolation valve NResearch SH360T042 Precleaned Volatile Organic Analyte (VOA) Sampling Vials Restek 21,797 Capacitive touch sensor Sparkfun SEN-1024 Pinch valve Valcor SV74P61T e1 Cell Reports Methods 2, 100233, June 20, 2022 Report ll OPEN ACCESS


    Article Title: Monitoring the oxidation of almond oils by HS-SPME–GC–MS and ATR-FTIR: Application of volatile compounds determination to cultivar authenticity
    Article Snippet: In this study, the oxidative process of Spanish and American almond oils was monitored by using headspace solid-phase microextraction/gas chromatography–mass spectrometry (HS-SPME/GC–MS) and attenuated total reflectance Fourier transform infrared spectroscopy (ATR-FTIR).. Oxidative stability of samples was evaluated after thermal treatment at 100 C for 1, 3, 5, 7, 10, 15 and 20 days, in order to accelerate the lipid oxidation process.. Variations observed in bands of infrared spectra were used to monitor the progress of the oxidation process of almond oils.



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    Figure 3. Activity assays for FDHZE (A) and AmDHZE (B). FDHZE activity on supraparticles is shown for varying formate concentrations. AmDHZE activity is shown for both free enzyme and the supraparticle-bound condition at several concentrations of <t>5M2H.</t>
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    Figure 3. Activity assays for FDHZE (A) and AmDHZE (B). FDHZE activity on supraparticles is shown for varying formate concentrations. AmDHZE activity is shown for both free enzyme and the supraparticle-bound condition at several concentrations of 5M2H.

    Journal: Biotechnology and bioengineering

    Article Title: Protein-inorganic calcium-phosphate supraparticles as a robust platform for enzyme co-immobilization.

    doi: 10.1002/bit.27348

    Figure Lengend Snippet: Figure 3. Activity assays for FDHZE (A) and AmDHZE (B). FDHZE activity on supraparticles is shown for varying formate concentrations. AmDHZE activity is shown for both free enzyme and the supraparticle-bound condition at several concentrations of 5M2H.

    Article Snippet: The 5- methyl-2-hexanone (5M2H) and benzoyl chloride (BzCl) were purchased from Alfa Aesar.

    Techniques: Activity Assay

    Figure 7. Conversion time courses of 5M2H to 5M2HAm as measured by HPLC.

    Journal: Biotechnology and bioengineering

    Article Title: Protein-inorganic calcium-phosphate supraparticles as a robust platform for enzyme co-immobilization.

    doi: 10.1002/bit.27348

    Figure Lengend Snippet: Figure 7. Conversion time courses of 5M2H to 5M2HAm as measured by HPLC.

    Article Snippet: The 5- methyl-2-hexanone (5M2H) and benzoyl chloride (BzCl) were purchased from Alfa Aesar.

    Techniques: