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Siemens AG smart ccd diffractometer
Smart Ccd Diffractometer, supplied by Siemens AG, used in various techniques. Bioz Stars score: 90/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
https://www.bioz.com/product/smart+diffractometer/smart+ccd+diffractometer/pmc02971113-6-1-0
Average 90 stars, based on 1 article reviews
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Article Title: Structural characterization of three semi-rigid tetracarboxylate-containing transition-metal coordination polymers
Article Snippet: Under hydro(solvo)thermal conditions, the reactions between transition-metal salts and tetracarboxylic acid molecules, with the assistance of organic base molecules, created three new coordination polymers, namely [H2(bpp)]2[Zn2(sph)2] H2O (sph = 4,40-sulfonediphthalate, bpp = 1,3-bis(piperidyl)propane) 1, [H2(bpp)]2[Ni2(oph)2(H2O)2] 2H2O (oph = 4,40-oxydiphthalate) 2 and [H2(bpe)]2[Ni(Hfph)2(bpe)] (bpe = 1,2-bis(pyridyl)ethylene; fph = 4,40-(hexafluoroisopropylidene)diphthalate) 3.. X-ray single-crystal diffraction analysis reveals that (i) in 1, the diprotonated bpp molecule acts as a templating agent.. The quadruple-bridged sph molecules propagate the tetrahedral Zn ions into a 2-D layer network in 1, where two types of circle loops are found; (ii) in 2, the bpp molecule is also diprotonated.

Article Title: Two novel penetrating coordination polymers based on flexible S-containing dicarboxylate acid with sensing properties towards Fe3+ and Cr2O72- ions
Article Snippet: Two new coordination polymers (CPs), namely, {*Zn(L)(bpp)+∙DMF}n (1) and {[Zn(L)(bpe)+∙DMF-n (2) (L = 2,2'-[benzene-1,3-diylbis(methanediylsulfanediyl)]dibenzoic acid, bpp= 1,3-bis(4-pyridyl)propane, bpe = 1,2-Bis(4-pyridyl)ethylene, DMF = N,N-Dimethylformamide), have been solvothermally synthesized and fully characterized.. Complex 1 displays a 2D→2D three-fold“false” interpenetrating structure while complex 2 possesses a novel 3-D 4-connected structure with fascinating self-penetrating moieties.. The luminescence studies reveal that these complexes exhibited excellent selectivity for Fe and Cr2O7 2ions in DMF.

Article Title: Growth and spectroscopic investigations of disordered Li3Ba2Yb3(MoO4)8 crystal
Article Snippet: 0925-3467/$ see front matter 2012 Elsevier B.V. A http://dx.doi.org/10.1016/j.optmat.2012.03.027 ⇑ Corresponding author.. E-mail address: smj521@hotmail.com (M. Song).. A large and transparent Li3Ba2Yb3(MoO4)8 crystal has been grown from a Li2MoO4 flux by the top seeded solution growth (TSSG) method.

Article Title: Crystal structure, thermal decomposition, mechanical sensitivity of Na[CL-14·2H2O] and its catalytic effect on the thermal decomposition of ammonium nitrate
Article Snippet: Please note that technical editing may introduce minor changes to the text and/or graphics, which may alter content.. The journal’s standard Terms & Conditions and the Ethical guidelines still apply.. In no event shall the Royal Society of Chemistry be held responsible for any errors or omissions in this Accepted Manuscript or any consequences arising from the use of any information it contains.

Article Title: Synthesis, Characterization, and Structure of Ruthenium Complex Ru(dppe)2C2O4 (dppe = Ph2P(CH2)2PPh2)
Article Snippet: Synthesis, Characterization, and Structure of Ruthenium Complex Ru(dppe)2C2O4 (dppe = Ph2P(CH2)2PPh2) Yi-Feng Zhou a , Li-Hong Huang a , Xiao-Hong Chen b , Ji-Dong Lou a & Xiu Lian Lu a a College of Life Sciences , China Jiliang University , Hangzhou , Zhejiang , P. R. China b State Key Laboratory of Chemical Engineering , Beijing University of Chemical Technology , Beijing , P. R. China Published online: 14 May 2013.

Article Title: N , N , N ′, N ′-Tetra­kis(pyridin-4-yl)methane­diamine monohydrate
Article Snippet: Siemens SMART CCD diffractometer Absorption correction: multi-scan ( SADABS ; Sheldrick, 1996 ) T min = 0.973, T max = 0.978 6540 measured reflections 2241 independent reflections 1313 reflections with I > 2σ( I ) R int = 0.033

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Article Title: (18-Crown-6)potassium [(1,2,5,6-η)-cycloocta-1,5-diene][(1,2,3,4-η)-naphthalene]ferrate(−I)
Article Snippet: .. Experimental Crystal data [K(C12H24O6)][Fe(C8H12)(C10H8)] Mr = 595.60 Triclinic, P1 a = 9.244 (1) Å b = 10.5285 (12) Å c = 15.971 (2) Å = 76.085 (2) = 89.651 (2) = 74.949 (2) V = 1454.4 (3) Å3 Z = 2 Mo K radiation = 0.70 mm 1 T = 173 K 0.42 0.32 0.22 mm Data collection Siemens SMART CCD diffractometer Absorption correction: multi-scan (SADABS; Sheldrick, 2008a) Tmin = 0.666, Tmax = 0.746 17413 measured reflections 6610 independent reflections 5576 reflections with I > 2 (I) Rint = 0.025 Refinement R[F 2 > 2 (F 2)] = 0.031 wR(F 2) = 0.073 S = 1.04 6610 reflections 423 parameters H atoms treated by a mixture of independent and constrained refinement max = 0.32 e Å 3 min = 0.29 e Å 3 Data collection: SMART (Bruker, 2003); cell refinement: SAINT (Bruker, 2003); data reduction: SAINT; program(s) used to solve structure: SIR97 (Altomare et al., 1999); program(s) used to refine structure: SHELXL97 (Sheldrick, 2008b); molecular graphics: SHELXTL (Sheldrick, 2008b); software used to prepare material for publication: SHELXTL. ..

Article Title: Synthesis and photoluminescence properties of rhenium(I) complexes based on 2,2':6',2''-terpyridine derivatives with hole-transporting units.
Article Snippet: Based on 2,2’:6’,2’’-terpyridine ligands (L1), five terpyridine derivatives, namely 4’-carbazol-9-yl-2,2’: 6’,2’’-terpyridine (L2), 4’-diphenylamino-2,2’:6’,2’’-terpyridine (L3), 4’-bis(4-tert-butylphenyl)amino2,2’:6’,2’’-terpyridine (L4), 4’-[naphthalen-1-yl-(phenyl)amino]-2,2’:6’,2’’-terpyridine (L5), 4’-[naphthalen2-yl(phenyl)amino]-2,2’:6’,2’’-terpyridine (L6) and their corresponding Re(I) complexes ReL(CO)3Cl (n = 1–6) have been synthesized and characterized by elemental analysis and H NMR spectroscopy.. The X-ray crystal structure of ReL3(CO)3Cl has also been obtained.. The luminescence spectra of ReL2(CO)3Cl–ReL5 (CO)3Cl, obtained in CH2Cl2 solution at room temperature, show strong dπ (Re) → π* (diimine) MLCT character (λmax ∼ 600 nm) and a small red shift relative to ReL1(CO)3Cl.



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