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    Millipore sabinene hydrate
    Synthesis of <t>4-Thujanol</t> Stereoisomers
    Sabinene Hydrate, supplied by Millipore, used in various techniques. Bioz Stars score: 93/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
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    Synthesis of 4-Thujanol Stereoisomers

    Journal: Journal of Natural Products

    Article Title: Asymmetric Synthesis of Oxygenated Monoterpenoids of Importance for Bark Beetle Ecology

    doi: 10.1021/acs.jnatprod.0c00669

    Figure Lengend Snippet: Synthesis of 4-Thujanol Stereoisomers

    Article Snippet: The commercial (+)-trans -4-thujanol ( 15 ) (Sigma-Aldrich) had a specific rotation of +29.8 (c 0.5, DCM).

    Techniques:

    Chromatograms of chiral-phase GC of 4-thujanol isomers in the mixture and chromatograms of isolated (+)- trans- and (−)- cis -4-thujanol isomers. The temperature program: Initial oven temp 40 °C (hold for 3 min) and increased to 150 °C at 3 °C/min and finally increased to 250 °C at 15 °C/min. It was kept for 10 min at the final temperature of 250 °C.

    Journal: Journal of Natural Products

    Article Title: Asymmetric Synthesis of Oxygenated Monoterpenoids of Importance for Bark Beetle Ecology

    doi: 10.1021/acs.jnatprod.0c00669

    Figure Lengend Snippet: Chromatograms of chiral-phase GC of 4-thujanol isomers in the mixture and chromatograms of isolated (+)- trans- and (−)- cis -4-thujanol isomers. The temperature program: Initial oven temp 40 °C (hold for 3 min) and increased to 150 °C at 3 °C/min and finally increased to 250 °C at 15 °C/min. It was kept for 10 min at the final temperature of 250 °C.

    Article Snippet: The commercial (+)-trans -4-thujanol ( 15 ) (Sigma-Aldrich) had a specific rotation of +29.8 (c 0.5, DCM).

    Techniques: Isolation

    1 H NMR spectrum of pondberry essential oil and identified major components of the oil (CDCl 3 , 400 MHz). (i) ( E )-β-ocimene, (ii) sabinene, (iii) α-phellandrene, (iv) limonene, (v) p -cymene, (vi) myrcene.

    Journal: Phytochemistry

    Article Title: Natural product studies of U.S. endangered plants: Volatile components of Lindera melissifolia (Lauraceae) repel mosquitoes and ticks

    doi: 10.1016/j.phytochem.2012.05.001

    Figure Lengend Snippet: 1 H NMR spectrum of pondberry essential oil and identified major components of the oil (CDCl 3 , 400 MHz). (i) ( E )-β-ocimene, (ii) sabinene, (iii) α-phellandrene, (iv) limonene, (v) p -cymene, (vi) myrcene.

    Article Snippet: N , N -Diethyl- 3-methylbenzamide (DEET) and trans -sabinene hydrate used for the tick and mosquito assays were purchased from Sigma–Aldrich, Inc., St. Louis, MO.

    Techniques: Nuclear Magnetic Resonance