Structured Review

Phenomenex libertellenone m separation
Structures of pimarane diterpenoids; myrocin F ( 1 ), <t>libertellenone</t> M ( 2 ), the suggested opened γ-lactone of libertellenone M ( 3 ), libertellenone C ( 4 ), and libertellenone E ( 5 ).
Libertellenone M Separation, supplied by Phenomenex, used in various techniques. Bioz Stars score: 91/100, based on 2 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
https://www.bioz.com/result/libertellenone m separation/product/Phenomenex
Average 91 stars, based on 2 article reviews
Price from $9.99 to $1999.99
libertellenone m separation - by Bioz Stars, 2020-08
91/100 stars

Images

1) Product Images from "A Dereplication and Bioguided Discovery Approach to Reveal New Compounds from a Marine-Derived Fungus Stilbella fimetaria"

Article Title: A Dereplication and Bioguided Discovery Approach to Reveal New Compounds from a Marine-Derived Fungus Stilbella fimetaria

Journal: Marine Drugs

doi: 10.3390/md15080253

Structures of pimarane diterpenoids; myrocin F ( 1 ), libertellenone M ( 2 ), the suggested opened γ-lactone of libertellenone M ( 3 ), libertellenone C ( 4 ), and libertellenone E ( 5 ).
Figure Legend Snippet: Structures of pimarane diterpenoids; myrocin F ( 1 ), libertellenone M ( 2 ), the suggested opened γ-lactone of libertellenone M ( 3 ), libertellenone C ( 4 ), and libertellenone E ( 5 ).

Techniques Used:

Selected key NOESY correlations for libertellenone M ( 2 ).
Figure Legend Snippet: Selected key NOESY correlations for libertellenone M ( 2 ).

Techniques Used:

2) Product Images from "A Dereplication and Bioguided Discovery Approach to Reveal New Compounds from a Marine-Derived Fungus Stilbella fimetaria"

Article Title: A Dereplication and Bioguided Discovery Approach to Reveal New Compounds from a Marine-Derived Fungus Stilbella fimetaria

Journal: Marine Drugs

doi: 10.3390/md15080253

Structures of pimarane diterpenoids; myrocin F ( 1 ), libertellenone M ( 2 ), the suggested opened γ-lactone of libertellenone M ( 3 ), libertellenone C ( 4 ), and libertellenone E ( 5 ).
Figure Legend Snippet: Structures of pimarane diterpenoids; myrocin F ( 1 ), libertellenone M ( 2 ), the suggested opened γ-lactone of libertellenone M ( 3 ), libertellenone C ( 4 ), and libertellenone E ( 5 ).

Techniques Used:

Selected key NOESY correlations for libertellenone M ( 2 ).
Figure Legend Snippet: Selected key NOESY correlations for libertellenone M ( 2 ).

Techniques Used:

Related Articles

High Performance Liquid Chromatography:

Article Title: A Dereplication and Bioguided Discovery Approach to Reveal New Compounds from a Marine-Derived Fungus Stilbella fimetaria
Article Snippet: .. Libertellenone M and the opened γ-lactone of libertellenone M separation was achieved on a Gemini C6 -Phenyl, 5 μm, 250 × 10 mm column (Phenomenex, Torrance, CA, USA) with a flow rate of 4 mL/min using a linear gradient 40% MeCN in Milli-Q water with 20 mM FA going to 100% MeCN in 28 min. Further libertellenone M separation was done on a Luna II C18 , 5 μm, 250 × 10 mm column (Phenomenex, Torrance, CA, USA) with a flow rate of 4 mL/min isocratic 55% MeCN in Milli-Q water with 20 mM FA in 20 min and a Kinetex Biphenyl, 5 μm 250 × 10 mm column (Phenomenex, Torrance, CA, USA) with a flow rate of 4 mL/min using a linear gradient 30% MeCN in Milli-Q water with 20 mM FA going to 100% MeCN in 25 min. Libertellenone C separation was achieved on a Luna II C18 , 5 μm, 250 × 10 mm column (Phenomenex, Torrance, CA, USA) with a flow rate of 5 mL/min using a linear gradient of 30% MeCN in Milli-Q water with 20 mM FA going to 70% MeCN in 30 min. Libertellenone E was purified from the EtOAc 3:1 MeOH fraction on the Waters 600 semipreparative HPLC. .. Separation was achieved on a Luna II C18 , 5 μm, 250 × 10 mm column (Phenomenex, Torrance, CA, USA) with a flow rate of 5 mL/min using a linear gradient of 30% MeCN in Milli-Q water with 20 mM FA going to 70% MeCN in 20 min and a Kinetex Biphenyl, 5 μm 250 × 10 mm column (Phenomenex, Torrance, CA, USA ) with a flow rate of 4 mL/min using a linear gradient of 30% MeCN in Milli-Q water with 20 mM FA going to 100% MeCN in 25 min. Cultivation 3: Extraction was achieved using 150 mL EtOAc per flask.

Flow Cytometry:

Article Title: A Dereplication and Bioguided Discovery Approach to Reveal New Compounds from a Marine-Derived Fungus Stilbella fimetaria
Article Snippet: .. Libertellenone M and the opened γ-lactone of libertellenone M separation was achieved on a Gemini C6 -Phenyl, 5 μm, 250 × 10 mm column (Phenomenex, Torrance, CA, USA) with a flow rate of 4 mL/min using a linear gradient 40% MeCN in Milli-Q water with 20 mM FA going to 100% MeCN in 28 min. Further libertellenone M separation was done on a Luna II C18 , 5 μm, 250 × 10 mm column (Phenomenex, Torrance, CA, USA) with a flow rate of 4 mL/min isocratic 55% MeCN in Milli-Q water with 20 mM FA in 20 min and a Kinetex Biphenyl, 5 μm 250 × 10 mm column (Phenomenex, Torrance, CA, USA) with a flow rate of 4 mL/min using a linear gradient 30% MeCN in Milli-Q water with 20 mM FA going to 100% MeCN in 25 min. Libertellenone C separation was achieved on a Luna II C18 , 5 μm, 250 × 10 mm column (Phenomenex, Torrance, CA, USA) with a flow rate of 5 mL/min using a linear gradient of 30% MeCN in Milli-Q water with 20 mM FA going to 70% MeCN in 30 min. Libertellenone E was purified from the EtOAc 3:1 MeOH fraction on the Waters 600 semipreparative HPLC. .. Separation was achieved on a Luna II C18 , 5 μm, 250 × 10 mm column (Phenomenex, Torrance, CA, USA) with a flow rate of 5 mL/min using a linear gradient of 30% MeCN in Milli-Q water with 20 mM FA going to 70% MeCN in 20 min and a Kinetex Biphenyl, 5 μm 250 × 10 mm column (Phenomenex, Torrance, CA, USA ) with a flow rate of 4 mL/min using a linear gradient of 30% MeCN in Milli-Q water with 20 mM FA going to 100% MeCN in 25 min. Cultivation 3: Extraction was achieved using 150 mL EtOAc per flask.

Purification:

Article Title: A Dereplication and Bioguided Discovery Approach to Reveal New Compounds from a Marine-Derived Fungus Stilbella fimetaria
Article Snippet: .. Libertellenone M and the opened γ-lactone of libertellenone M separation was achieved on a Gemini C6 -Phenyl, 5 μm, 250 × 10 mm column (Phenomenex, Torrance, CA, USA) with a flow rate of 4 mL/min using a linear gradient 40% MeCN in Milli-Q water with 20 mM FA going to 100% MeCN in 28 min. Further libertellenone M separation was done on a Luna II C18 , 5 μm, 250 × 10 mm column (Phenomenex, Torrance, CA, USA) with a flow rate of 4 mL/min isocratic 55% MeCN in Milli-Q water with 20 mM FA in 20 min and a Kinetex Biphenyl, 5 μm 250 × 10 mm column (Phenomenex, Torrance, CA, USA) with a flow rate of 4 mL/min using a linear gradient 30% MeCN in Milli-Q water with 20 mM FA going to 100% MeCN in 25 min. Libertellenone C separation was achieved on a Luna II C18 , 5 μm, 250 × 10 mm column (Phenomenex, Torrance, CA, USA) with a flow rate of 5 mL/min using a linear gradient of 30% MeCN in Milli-Q water with 20 mM FA going to 70% MeCN in 30 min. Libertellenone E was purified from the EtOAc 3:1 MeOH fraction on the Waters 600 semipreparative HPLC. .. Separation was achieved on a Luna II C18 , 5 μm, 250 × 10 mm column (Phenomenex, Torrance, CA, USA) with a flow rate of 5 mL/min using a linear gradient of 30% MeCN in Milli-Q water with 20 mM FA going to 70% MeCN in 20 min and a Kinetex Biphenyl, 5 μm 250 × 10 mm column (Phenomenex, Torrance, CA, USA ) with a flow rate of 4 mL/min using a linear gradient of 30% MeCN in Milli-Q water with 20 mM FA going to 100% MeCN in 25 min. Cultivation 3: Extraction was achieved using 150 mL EtOAc per flask.

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    Phenomenex libertellenone m separation
    Structures of pimarane diterpenoids; myrocin F ( 1 ), <t>libertellenone</t> M ( 2 ), the suggested opened γ-lactone of libertellenone M ( 3 ), libertellenone C ( 4 ), and libertellenone E ( 5 ).
    Libertellenone M Separation, supplied by Phenomenex, used in various techniques. Bioz Stars score: 91/100, based on 2 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
    https://www.bioz.com/result/libertellenone m separation/product/Phenomenex
    Average 91 stars, based on 2 article reviews
    Price from $9.99 to $1999.99
    libertellenone m separation - by Bioz Stars, 2020-08
    91/100 stars
      Buy from Supplier

    Image Search Results


    Structures of pimarane diterpenoids; myrocin F ( 1 ), libertellenone M ( 2 ), the suggested opened γ-lactone of libertellenone M ( 3 ), libertellenone C ( 4 ), and libertellenone E ( 5 ).

    Journal: Marine Drugs

    Article Title: A Dereplication and Bioguided Discovery Approach to Reveal New Compounds from a Marine-Derived Fungus Stilbella fimetaria

    doi: 10.3390/md15080253

    Figure Lengend Snippet: Structures of pimarane diterpenoids; myrocin F ( 1 ), libertellenone M ( 2 ), the suggested opened γ-lactone of libertellenone M ( 3 ), libertellenone C ( 4 ), and libertellenone E ( 5 ).

    Article Snippet: Libertellenone M and the opened γ-lactone of libertellenone M separation was achieved on a Gemini C6 -Phenyl, 5 μm, 250 × 10 mm column (Phenomenex, Torrance, CA, USA) with a flow rate of 4 mL/min using a linear gradient 40% MeCN in Milli-Q water with 20 mM FA going to 100% MeCN in 28 min. Further libertellenone M separation was done on a Luna II C18 , 5 μm, 250 × 10 mm column (Phenomenex, Torrance, CA, USA) with a flow rate of 4 mL/min isocratic 55% MeCN in Milli-Q water with 20 mM FA in 20 min and a Kinetex Biphenyl, 5 μm 250 × 10 mm column (Phenomenex, Torrance, CA, USA) with a flow rate of 4 mL/min using a linear gradient 30% MeCN in Milli-Q water with 20 mM FA going to 100% MeCN in 25 min. Libertellenone C separation was achieved on a Luna II C18 , 5 μm, 250 × 10 mm column (Phenomenex, Torrance, CA, USA) with a flow rate of 5 mL/min using a linear gradient of 30% MeCN in Milli-Q water with 20 mM FA going to 70% MeCN in 30 min. Libertellenone E was purified from the EtOAc 3:1 MeOH fraction on the Waters 600 semipreparative HPLC.

    Techniques:

    Selected key NOESY correlations for libertellenone M ( 2 ).

    Journal: Marine Drugs

    Article Title: A Dereplication and Bioguided Discovery Approach to Reveal New Compounds from a Marine-Derived Fungus Stilbella fimetaria

    doi: 10.3390/md15080253

    Figure Lengend Snippet: Selected key NOESY correlations for libertellenone M ( 2 ).

    Article Snippet: Libertellenone M and the opened γ-lactone of libertellenone M separation was achieved on a Gemini C6 -Phenyl, 5 μm, 250 × 10 mm column (Phenomenex, Torrance, CA, USA) with a flow rate of 4 mL/min using a linear gradient 40% MeCN in Milli-Q water with 20 mM FA going to 100% MeCN in 28 min. Further libertellenone M separation was done on a Luna II C18 , 5 μm, 250 × 10 mm column (Phenomenex, Torrance, CA, USA) with a flow rate of 4 mL/min isocratic 55% MeCN in Milli-Q water with 20 mM FA in 20 min and a Kinetex Biphenyl, 5 μm 250 × 10 mm column (Phenomenex, Torrance, CA, USA) with a flow rate of 4 mL/min using a linear gradient 30% MeCN in Milli-Q water with 20 mM FA going to 100% MeCN in 25 min. Libertellenone C separation was achieved on a Luna II C18 , 5 μm, 250 × 10 mm column (Phenomenex, Torrance, CA, USA) with a flow rate of 5 mL/min using a linear gradient of 30% MeCN in Milli-Q water with 20 mM FA going to 70% MeCN in 30 min. Libertellenone E was purified from the EtOAc 3:1 MeOH fraction on the Waters 600 semipreparative HPLC.

    Techniques: