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Image Search Results
Journal: Journal of Analytical Toxicology
Article Title: Toward the Interpretation of Positive Testing for Fentanyl and Its Analogs in Real Hair Samples: Preliminary Considerations
doi: 10.1093/jat/bkz102
Figure Lengend Snippet: Summary of Results Obtained from 293 Real Hair Samples
Article Snippet: Reagents and standards Reagents and standards for
Techniques:
Journal: ACS Omega
Article Title: LC-MS/MS-Based Method for the Multiplex Detection of 24 Fentanyl Analogues and Metabolites in Whole Blood at Sub ng mL –1 Concentrations
doi: 10.1021/acsomega.7b01536
Figure Lengend Snippet: LC-MS/MS ion chromatogram of a high calibrator. Each peak represents the quantitative transition ion (qualitative transition ion not shown). Fentanyl analogue and internal standard peak identities: (1) norfentanyl- d 5 , (2) norfentanyl, (3) furanyl norfentanyl, (4) remifentanil acid, (5) butyryl norfentanyl, (6) remifentanil, (7) acetyl fentanyl, (8) acetyl fentanyl- 13 C 6 , (9) alfentanil, (10) U-47700, (11) acetyl fentanyl 4-methylphenethyl, (12) acrylfentanyl, (13) fentanyl, (14) AH-7921, (15) fentanyl- d 5 , (16) 4-ANPP, (17) para -methoxyfentanyl, (18) furanyl fentanyl, (19) despropionyl para -fluorofentanyl, (20) (±)- cis -3-methyl fentanyl, (21) butyryl/isobutyryl fentanyl, (22) carfentanil, (23) para -fluorobutyryl/ para -fluoroisobutyryl fentanyl, (24) sufentanil, and (25) valeryl fentanyl. Separation between butyryl/isobutyryl and para -fluoroisobutyryl fentanyl/ para -fluorobutyryl fentanyl was not achieved due to isomerism.
Article Snippet: Internal standards were
Techniques: Liquid Chromatography with Mass Spectroscopy
Journal: ACS Omega
Article Title: LC-MS/MS-Based Method for the Multiplex Detection of 24 Fentanyl Analogues and Metabolites in Whole Blood at Sub ng mL –1 Concentrations
doi: 10.1021/acsomega.7b01536
Figure Lengend Snippet: Quantitative ion chromatogram of an accidental overdose case from late 2016. Abbreviations are as follows: (1) norfentanyl- d 5 , (2) norfentanyl, (8) acetyl fentanyl 13 C 6 , (10) U-47700, (13) fentanyl, (15) fentanyl- d 5 , (16) 4-ANPP, (18) furanyl fentanyl, (19) despropionyl para -fluorofentanyl, (21) butyryl/isobutyryl fentanyl, and (23) para -fluorobutyryl/ para -fluoroisobutyryl fentanyl. Inset shows the low-response count region of IMF analogues.
Article Snippet: Internal standards were
Techniques:
Journal: Analytical and Bioanalytical Chemistry
Article Title: Conductive vial electromembrane extraction of opioids from oral fluid
doi: 10.1007/s00216-023-04807-3
Figure Lengend Snippet: Validation data of opioids: coefficient of correlation ( R ), precision (CV%), and accuracy (bias%) at the lower limit of quantification (LLOQ) and three QC levels, recoveries (RE), matrix effects (ME), and internal standard corrected matrix effects. The quantification range was from LLOQ to 50 × LLOQ for all analytes
Article Snippet: Codeine,
Techniques: Concentration Assay