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Statistics for diffraction data collection and processing.

Journal: Journal of immunology (Baltimore, Md. : 1950)

Article Title: Crystal structure of the labile complex of interleukin 24 (IL-24) with the extracellular domains of IL-22R1 and IL-20R2

doi: 10.4049/jimmunol.1800726

Figure Lengend Snippet: Statistics for diffraction data collection and processing.

Article Snippet: Detailed characteristics of the final model are shown in . table ft1 table-wrap mode="anchored" t5 Table 1. caption a7 Diffraction source Beamline 22-ID, SER-CAT, APS, ANL, IL, USA Wavelength (Å) 1.0000 Temperature (K) 100 Detector Rayonix 300HS high speed CCD Crystal-to-detector distance (mm) 270 Rotation range per image (°) 1.0 Total rotation range (°) 360 Exposure time per image (s) 1.0 Space group P 4 3 a, b, c (Å) 77.70, 77.70, 124.79 Mosaicity (°) 0.25 – 0.90 Resolution range (Å) 99.00 – 2.15 (2.23 –2.15) * Total No. of reflections 317,252 No. of unique reflections 39,903 Completeness (%) 99.7 (100) Multiplicity 8.0 (7.1) 29.7 (1.62) R merge † 0.072 (1.416) R p.i.m ‡ 0.034 (0.62) CC 1/2 0.97 (0.70) Open in a separate window * Values in parentheses are for the highest resolution shell.

Techniques:

Journal: Clinical Mass Spectrometry

Article Title: Mass spectrometry for therapeutic drug monitoring of anti-tuberculosis drugs

doi: 10.1016/j.clinms.2018.10.002

Figure Lengend Snippet: Multi-analyte assays for first- and second-line anti-tuberculosis drugs and single -analyte assays for second-line drugs using LC-MS/MS.

Article Snippet: R, H, E, Z, S [47] , Phenacetin , >18 , 100, plasma , methanol, formic acid , Agilent, Zorbax SB-C18 (100 × 2.1 mm, 3.5 μm) , R, Z 0.2–4, H 0.08–2, E 0.0002–1, S 0.002–0.2 , A: 0.02% heptaflourobutyric acid, 0.2% formic acid in methanol B: 0.02% heptaflourobutyric acid, 0.2% formic acid in water pH: NA , 8.5 , R ca 7.2, H ca 1.3, E ca 1.6, Z ca 1.7, S ca 1.5 , R 823.4–791.2, H 138.1–120.9, E 205.3–116.2 Z 124.1–79.1, S 582.3–262.6.

Techniques: Hydrophilic Interaction Liquid Chromatography