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1 3 dichloro 1 1 3 3 tetraisopropyldisiloxane  (Chem Impex International)


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    Chem Impex International 1 3 dichloro 1 1 3 3 tetraisopropyldisiloxane
    1 3 Dichloro 1 1 3 3 Tetraisopropyldisiloxane, supplied by Chem Impex International, used in various techniques. Bioz Stars score: 91/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
    https://www.bioz.com/result/1 3 dichloro 1 1 3 3 tetraisopropyldisiloxane/product/Chem Impex International
    Average 91 stars, based on 1 article reviews
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    91/100 stars

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    Chem Impex International 1 3 dichloro 1 1 3 3 tetraisopropyldisiloxane
    1 3 Dichloro 1 1 3 3 Tetraisopropyldisiloxane, supplied by Chem Impex International, used in various techniques. Bioz Stars score: 91/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
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    Thermo Fisher 1 3 dichloro 1 1 3 3 tetraisopropyldisiloxane
    Reagents and conditions: a) <t>1,3-dichloro-1,1,3,3-tetraisopropyldisiloxane,</t> pyridine, overnight, 75%; b) beta-D-ribofuranose 1-acetate 2,3,5-tribenzoate, SnCl 4 , DCE, 30 h, 70%; c) TBAF, THF, 30 min, 80%; d) DMTrCl, pyridine, 2 h; e) TBSCl, imidazole, 2 h, two-step yield 61%; f) PTSA, CHCl 3 /MeOH, 10 min, 91%; g) dibenzyl diisopropylphosphoramidite, 4,5-dicyanoimidazole, TBHP, CH 2 Cl 2 /MeCN, 4.5 h, 71%; h) NH 3 /MeOH, 24 h, 80%; i) DMTrCl, pyridine, 2 h; j) TBSCl, imidazole, 2 h; k) p -toluenesulfonic acid monohydrate, CHCl 3 /MeOH, 10 min, three-step yield 58%; l) dibenzyl diisopropylphosphoramidite, 4,5-dicyanoimidazole, TBHP, CH 2 Cl 2 /MeCN, 4.5 h, 69%; m) TBAF, THF, 30 min; n) Pd/C, Et 3 N, H 2 , t -BuOH/H 2 O, two-step yield 50%.
    1 3 Dichloro 1 1 3 3 Tetraisopropyldisiloxane, supplied by Thermo Fisher, used in various techniques. Bioz Stars score: 86/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
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    86
    Millipore 1 3 dichloro 1 1 3 3 tetraisopropyldisiloxane
    Reagents and conditions: a) <t>1,3-dichloro-1,1,3,3-tetraisopropyldisiloxane,</t> pyridine, overnight, 75%; b) beta-D-ribofuranose 1-acetate 2,3,5-tribenzoate, SnCl 4 , DCE, 30 h, 70%; c) TBAF, THF, 30 min, 80%; d) DMTrCl, pyridine, 2 h; e) TBSCl, imidazole, 2 h, two-step yield 61%; f) PTSA, CHCl 3 /MeOH, 10 min, 91%; g) dibenzyl diisopropylphosphoramidite, 4,5-dicyanoimidazole, TBHP, CH 2 Cl 2 /MeCN, 4.5 h, 71%; h) NH 3 /MeOH, 24 h, 80%; i) DMTrCl, pyridine, 2 h; j) TBSCl, imidazole, 2 h; k) p -toluenesulfonic acid monohydrate, CHCl 3 /MeOH, 10 min, three-step yield 58%; l) dibenzyl diisopropylphosphoramidite, 4,5-dicyanoimidazole, TBHP, CH 2 Cl 2 /MeCN, 4.5 h, 69%; m) TBAF, THF, 30 min; n) Pd/C, Et 3 N, H 2 , t -BuOH/H 2 O, two-step yield 50%.
    1 3 Dichloro 1 1 3 3 Tetraisopropyldisiloxane, supplied by Millipore, used in various techniques. Bioz Stars score: 86/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
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    AutoMate Scientific Inc 1 3 dichloro 1 1 3 3 tetraisopropyldisiloxane
    Reagents and conditions: a) <t>1,3-dichloro-1,1,3,3-tetraisopropyldisiloxane,</t> pyridine, overnight, 75%; b) beta-D-ribofuranose 1-acetate 2,3,5-tribenzoate, SnCl 4 , DCE, 30 h, 70%; c) TBAF, THF, 30 min, 80%; d) DMTrCl, pyridine, 2 h; e) TBSCl, imidazole, 2 h, two-step yield 61%; f) PTSA, CHCl 3 /MeOH, 10 min, 91%; g) dibenzyl diisopropylphosphoramidite, 4,5-dicyanoimidazole, TBHP, CH 2 Cl 2 /MeCN, 4.5 h, 71%; h) NH 3 /MeOH, 24 h, 80%; i) DMTrCl, pyridine, 2 h; j) TBSCl, imidazole, 2 h; k) p -toluenesulfonic acid monohydrate, CHCl 3 /MeOH, 10 min, three-step yield 58%; l) dibenzyl diisopropylphosphoramidite, 4,5-dicyanoimidazole, TBHP, CH 2 Cl 2 /MeCN, 4.5 h, 69%; m) TBAF, THF, 30 min; n) Pd/C, Et 3 N, H 2 , t -BuOH/H 2 O, two-step yield 50%.
    1 3 Dichloro 1 1 3 3 Tetraisopropyldisiloxane, supplied by AutoMate Scientific Inc, used in various techniques. Bioz Stars score: 86/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
    https://www.bioz.com/result/1 3 dichloro 1 1 3 3 tetraisopropyldisiloxane/product/AutoMate Scientific Inc
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    Millipore dichloro 1 1 3 3 tetraisopropyldisiloxane
    Reagents and conditions: a) <t>1,3-dichloro-1,1,3,3-tetraisopropyldisiloxane,</t> pyridine, overnight, 75%; b) beta-D-ribofuranose 1-acetate 2,3,5-tribenzoate, SnCl 4 , DCE, 30 h, 70%; c) TBAF, THF, 30 min, 80%; d) DMTrCl, pyridine, 2 h; e) TBSCl, imidazole, 2 h, two-step yield 61%; f) PTSA, CHCl 3 /MeOH, 10 min, 91%; g) dibenzyl diisopropylphosphoramidite, 4,5-dicyanoimidazole, TBHP, CH 2 Cl 2 /MeCN, 4.5 h, 71%; h) NH 3 /MeOH, 24 h, 80%; i) DMTrCl, pyridine, 2 h; j) TBSCl, imidazole, 2 h; k) p -toluenesulfonic acid monohydrate, CHCl 3 /MeOH, 10 min, three-step yield 58%; l) dibenzyl diisopropylphosphoramidite, 4,5-dicyanoimidazole, TBHP, CH 2 Cl 2 /MeCN, 4.5 h, 69%; m) TBAF, THF, 30 min; n) Pd/C, Et 3 N, H 2 , t -BuOH/H 2 O, two-step yield 50%.
    Dichloro 1 1 3 3 Tetraisopropyldisiloxane, supplied by Millipore, used in various techniques. Bioz Stars score: 86/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
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    Millipore dichloro 1 1 3 3 tetraisopropyldisiloxane ak scientific naphthylmethyl bromide aldrich tetra n butylammonium fluoride sigma aldrich
    Reagents and conditions: a) <t>1,3-dichloro-1,1,3,3-tetraisopropyldisiloxane,</t> pyridine, overnight, 75%; b) beta-D-ribofuranose 1-acetate 2,3,5-tribenzoate, SnCl 4 , DCE, 30 h, 70%; c) TBAF, THF, 30 min, 80%; d) DMTrCl, pyridine, 2 h; e) TBSCl, imidazole, 2 h, two-step yield 61%; f) PTSA, CHCl 3 /MeOH, 10 min, 91%; g) dibenzyl diisopropylphosphoramidite, 4,5-dicyanoimidazole, TBHP, CH 2 Cl 2 /MeCN, 4.5 h, 71%; h) NH 3 /MeOH, 24 h, 80%; i) DMTrCl, pyridine, 2 h; j) TBSCl, imidazole, 2 h; k) p -toluenesulfonic acid monohydrate, CHCl 3 /MeOH, 10 min, three-step yield 58%; l) dibenzyl diisopropylphosphoramidite, 4,5-dicyanoimidazole, TBHP, CH 2 Cl 2 /MeCN, 4.5 h, 69%; m) TBAF, THF, 30 min; n) Pd/C, Et 3 N, H 2 , t -BuOH/H 2 O, two-step yield 50%.
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    AutoMate Scientific Inc dichloro 1 1 3 3 tetraisopropyldisiloxane ak scientific naphthylmethyl bromide aldrich tetra n butylammonium fluoride sigma aldrich
    Reagents and conditions: a) <t>1,3-dichloro-1,1,3,3-tetraisopropyldisiloxane,</t> pyridine, overnight, 75%; b) beta-D-ribofuranose 1-acetate 2,3,5-tribenzoate, SnCl 4 , DCE, 30 h, 70%; c) TBAF, THF, 30 min, 80%; d) DMTrCl, pyridine, 2 h; e) TBSCl, imidazole, 2 h, two-step yield 61%; f) PTSA, CHCl 3 /MeOH, 10 min, 91%; g) dibenzyl diisopropylphosphoramidite, 4,5-dicyanoimidazole, TBHP, CH 2 Cl 2 /MeCN, 4.5 h, 71%; h) NH 3 /MeOH, 24 h, 80%; i) DMTrCl, pyridine, 2 h; j) TBSCl, imidazole, 2 h; k) p -toluenesulfonic acid monohydrate, CHCl 3 /MeOH, 10 min, three-step yield 58%; l) dibenzyl diisopropylphosphoramidite, 4,5-dicyanoimidazole, TBHP, CH 2 Cl 2 /MeCN, 4.5 h, 69%; m) TBAF, THF, 30 min; n) Pd/C, Et 3 N, H 2 , t -BuOH/H 2 O, two-step yield 50%.
    Dichloro 1 1 3 3 Tetraisopropyldisiloxane Ak Scientific Naphthylmethyl Bromide Aldrich Tetra N Butylammonium Fluoride Sigma Aldrich, supplied by AutoMate Scientific Inc, used in various techniques. Bioz Stars score: 86/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
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    Merck & Co dichloro 1 1 3 3 tetraisopropyldisiloxane ak scientific naphthylmethyl bromide aldrich tetra n butylammonium fluoride sigma aldrich
    Reagents and conditions: a) <t>1,3-dichloro-1,1,3,3-tetraisopropyldisiloxane,</t> pyridine, overnight, 75%; b) beta-D-ribofuranose 1-acetate 2,3,5-tribenzoate, SnCl 4 , DCE, 30 h, 70%; c) TBAF, THF, 30 min, 80%; d) DMTrCl, pyridine, 2 h; e) TBSCl, imidazole, 2 h, two-step yield 61%; f) PTSA, CHCl 3 /MeOH, 10 min, 91%; g) dibenzyl diisopropylphosphoramidite, 4,5-dicyanoimidazole, TBHP, CH 2 Cl 2 /MeCN, 4.5 h, 71%; h) NH 3 /MeOH, 24 h, 80%; i) DMTrCl, pyridine, 2 h; j) TBSCl, imidazole, 2 h; k) p -toluenesulfonic acid monohydrate, CHCl 3 /MeOH, 10 min, three-step yield 58%; l) dibenzyl diisopropylphosphoramidite, 4,5-dicyanoimidazole, TBHP, CH 2 Cl 2 /MeCN, 4.5 h, 69%; m) TBAF, THF, 30 min; n) Pd/C, Et 3 N, H 2 , t -BuOH/H 2 O, two-step yield 50%.
    Dichloro 1 1 3 3 Tetraisopropyldisiloxane Ak Scientific Naphthylmethyl Bromide Aldrich Tetra N Butylammonium Fluoride Sigma Aldrich, supplied by Merck & Co, used in various techniques. Bioz Stars score: 86/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
    https://www.bioz.com/result/dichloro 1 1 3 3 tetraisopropyldisiloxane ak scientific naphthylmethyl bromide aldrich tetra n butylammonium fluoride sigma aldrich/product/Merck & Co
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    Shin-Etsu Chemical Co Ltd 1 3 dichloro 1 1 3 3 tetraisopropyldisiloxane
    Reagents and conditions: a) <t>1,3-dichloro-1,1,3,3-tetraisopropyldisiloxane,</t> pyridine, overnight, 75%; b) beta-D-ribofuranose 1-acetate 2,3,5-tribenzoate, SnCl 4 , DCE, 30 h, 70%; c) TBAF, THF, 30 min, 80%; d) DMTrCl, pyridine, 2 h; e) TBSCl, imidazole, 2 h, two-step yield 61%; f) PTSA, CHCl 3 /MeOH, 10 min, 91%; g) dibenzyl diisopropylphosphoramidite, 4,5-dicyanoimidazole, TBHP, CH 2 Cl 2 /MeCN, 4.5 h, 71%; h) NH 3 /MeOH, 24 h, 80%; i) DMTrCl, pyridine, 2 h; j) TBSCl, imidazole, 2 h; k) p -toluenesulfonic acid monohydrate, CHCl 3 /MeOH, 10 min, three-step yield 58%; l) dibenzyl diisopropylphosphoramidite, 4,5-dicyanoimidazole, TBHP, CH 2 Cl 2 /MeCN, 4.5 h, 69%; m) TBAF, THF, 30 min; n) Pd/C, Et 3 N, H 2 , t -BuOH/H 2 O, two-step yield 50%.
    1 3 Dichloro 1 1 3 3 Tetraisopropyldisiloxane, supplied by Shin-Etsu Chemical Co Ltd, used in various techniques. Bioz Stars score: 86/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
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    Reagents and conditions: a) 1,3-dichloro-1,1,3,3-tetraisopropyldisiloxane, pyridine, overnight, 75%; b) beta-D-ribofuranose 1-acetate 2,3,5-tribenzoate, SnCl 4 , DCE, 30 h, 70%; c) TBAF, THF, 30 min, 80%; d) DMTrCl, pyridine, 2 h; e) TBSCl, imidazole, 2 h, two-step yield 61%; f) PTSA, CHCl 3 /MeOH, 10 min, 91%; g) dibenzyl diisopropylphosphoramidite, 4,5-dicyanoimidazole, TBHP, CH 2 Cl 2 /MeCN, 4.5 h, 71%; h) NH 3 /MeOH, 24 h, 80%; i) DMTrCl, pyridine, 2 h; j) TBSCl, imidazole, 2 h; k) p -toluenesulfonic acid monohydrate, CHCl 3 /MeOH, 10 min, three-step yield 58%; l) dibenzyl diisopropylphosphoramidite, 4,5-dicyanoimidazole, TBHP, CH 2 Cl 2 /MeCN, 4.5 h, 69%; m) TBAF, THF, 30 min; n) Pd/C, Et 3 N, H 2 , t -BuOH/H 2 O, two-step yield 50%.

    Journal: bioRxiv

    Article Title: Identification and receptor mechanism of TIR-catalyzed small molecules in plant immunity

    doi: 10.1101/2022.04.01.486681

    Figure Lengend Snippet: Reagents and conditions: a) 1,3-dichloro-1,1,3,3-tetraisopropyldisiloxane, pyridine, overnight, 75%; b) beta-D-ribofuranose 1-acetate 2,3,5-tribenzoate, SnCl 4 , DCE, 30 h, 70%; c) TBAF, THF, 30 min, 80%; d) DMTrCl, pyridine, 2 h; e) TBSCl, imidazole, 2 h, two-step yield 61%; f) PTSA, CHCl 3 /MeOH, 10 min, 91%; g) dibenzyl diisopropylphosphoramidite, 4,5-dicyanoimidazole, TBHP, CH 2 Cl 2 /MeCN, 4.5 h, 71%; h) NH 3 /MeOH, 24 h, 80%; i) DMTrCl, pyridine, 2 h; j) TBSCl, imidazole, 2 h; k) p -toluenesulfonic acid monohydrate, CHCl 3 /MeOH, 10 min, three-step yield 58%; l) dibenzyl diisopropylphosphoramidite, 4,5-dicyanoimidazole, TBHP, CH 2 Cl 2 /MeCN, 4.5 h, 69%; m) TBAF, THF, 30 min; n) Pd/C, Et 3 N, H 2 , t -BuOH/H 2 O, two-step yield 50%.

    Article Snippet: The mass spectra (MS, Thermo, LCQ, Fleet) were measured at the School of Pharmaceutical Sciences, Zhengzhou University Compound 2: To a stirring solution of 1 (30.00 g, 80.84 mmol) in pyridine (200 mL) at 0 °C was added 1,3-dichloro-1,1,3,3-tetraisopropyldisiloxane (26.77 g, 84.88 mmol), and the solution was stirred at room temperature for overnight.

    Techniques: